| NMR
Spectroscopy |
|
Instrumentation |
Capabilities |
| Varian
Inova500 |
Liquid phase,
multinuclear 3 channel with PFG capabilities |
| Bruker
AMX-500 |
Liquid phase,
multinuclear, inverse and spin locking capabilities, selective pulses |
|
Varian/Anasazi FT 90 |
Liquid phase,
proton and carbon (teaching labs) |
|
Homebuilt/Magnex 500 MHz |
Solid state,
triple resonance, CPMAS, CRAMPS |
| Varian 800
MHz
Collaboration with Brown Cancer Center |
|
|
EPR
Spectroscopy |
| Varian E-109
Century Series |
X-band
frequency, electronic and structural properties |
| Infrared Spectroscopy |
| Mattson 5020
FTIR Spectrometer |
DRIFTS
(diffuse reflectance) (4000-400 cm-1) |
| Mattson 8020
FTIR Spectrometer |
ATR
(attenuated total reflection) |
| Mattson RS-1
Configured for NIR |
Spectroelectrochemistry |
| Nicolet
Impact 410 FTIR Spectrometer |
Quick-IR and
OMNIC software (teaching labs) |
| Optical Polarimetry |
| Jasco DIP 370 |
|
| UV-Visible Spectroscopy |
| HP 8452A
diode array spectrophotometer |
Liquid and
film studies of electronic spectra
(200 - 800 nm) |
| Atomic Spectroscopies |
| Perkin-Elmer
flame AAS |
Solution
species single component analysis with ppm detection |
|
Gas Chromatography |
| 3 Gow Mac 350
GCs |
|
| GC-Mass Spectroscopy |
| HP 5890 GC
with 5971A |
Separate and
identify volatile organic components |
| HP 5890 GC
with HP5970 quadrupole MS |
Biomolecular Mass Spectrometry Laboratory |
|
Mass Spectrometry |
|
MALDI-TOF PE Biosystems Voyager DE-Pro |
Linear and
reflectron modes, delayed extraction, post-source decay, timed ion |
| Fourier
Transform-Ion Cyclotron Resonance-Mass Spectrometer (FT-ICR-MS) |
Thermo
LTQ-FT, which is an ion trap MS interfaced to a FT-ICR-MS with CID, ECD, and
IRMPD dissociation modes, with sources such as ESI, nanospray (including the
Nanomate) and Mass Tech
AP-MALDI-PDF |
| Thermo
X-Series Collision-Cell ICP-MS (Inductively Coupled Plasma Mass
Spectrometer) with New Wave 213 nm Laser Ablation System and Microsampler |
|
| Scanning Electron Microscopy |
| ISI with EDX
capabilities (Geology) |
Image
resolution to 1 & microm, elemental analyses to 1% (w/w) |
|
X-Ray
Crystallography |
| Rigaku Dmax B
(ChemE.) |
Powder
diffraction patterns |
| Bruker AXS
diffractometer with CCD detector |
Single
crystal diffractometry, Cu and Mo targets. Variable temperture range 90 K -
300 K |
| EN Guinier
camera |
Powder
diffraction patterns |
| Rigaku-MSC
RU-H3R Rotating Anode Generator with Mar345dtb X-ray detector |
Macromolecular X-ray Diffraction |
|
Molecular Modeling |
| Linux network
with six 4-processor and two 8-processor boxes running Gaussian 98, AMBER,
PQS and other quantum chemistry, statistical chemistry and graphics codes. |
Additionally,
there are Silicon Graphics computers running MSI software for computational
chemistry, surface science, NMR and other applications. These include two
O2s and one Octane. |
| Molecular
Modeling Facilites at the
Brown Cancer Center
|
